A sensitive HPLC-FLD method combined with multivariate analysis for the determination of amino acids in l-citrulline rich vegetables
Publication date: Available online 23 April 2019Source: Journal of Food and Drug AnalysisAuthor(s): Karen A. Corleto, Jashbir Singh, G.K. Jayaprakasha, Bhimanagouda S. PatilAbstractThe proposed analytical method reports the separation and quantification of 21 amino acids including l-citrulline from fresh vegetables and commercial juices using C8 column. Optimal separation conditions for amino acids analysis were obtained with 20 mM sodium acetate (solvent A) and water with organic modifier acetonitrile and methanol (solvent B; 18/50/32 V/V). The ideal pH and column temperature were found to be 5.40 and 35 °C, respectiv...
Source: Journal of Food and Drug Analysis - April 25, 2019 Category: Food Science Source Type: research

Editorial Board
Publication date: April 2019Source: Journal of Food and Drug Analysis, Volume 27, Issue 2Author(s): (Source: Journal of Food and Drug Analysis)
Source: Journal of Food and Drug Analysis - April 14, 2019 Category: Food Science Source Type: research

Detection of BPDE-DNA adducts in human umbilical cord blood by LC-MS/MS analysis
In this study, we employed our developed LC-MS/MS method to detect and quantity BPDE-dG adducts present in 42 normal human umbilical blood samples and 42 birth defect cases. We determined that there is no significant difference in the level of BPDE-dG formation between the normal and birth defect groups. This represents the first time to use an LC-MS/MS method to quantify BPDE-dG in human umbilical blood samples. The results indicated that under experimental conditions, BPDE-dG adducts were detected in all the human umbilical blood samples from the normal and birth defect groups.Graphical abstract (Source: Journal of Food and Drug Analysis)
Source: Journal of Food and Drug Analysis - March 24, 2019 Category: Food Science Source Type: research

Determination of phenylenediamines in hair colors derivatizated with 5-(4, 6-dichlorotriazinyl)aminofluorescein via micellar electrokinetic chromatography
Publication date: Available online 21 March 2019Source: Journal of Food and Drug AnalysisAuthor(s): Hung-Yu Ko, Yi-Hui Lin, Chi-Jen Shih, Yen-Ling ChenAbstractPhenylenediamines (PDs), which are reported to cause allergic dermatitis and possess genotoxicity and carcinogenicity, are the ingredients used in permanent hair dyes. The fluorescent derivatization strategy coupled with micellar electrokinetic chromatography (MEKC) were established to analyze four PDs, including o-phenylenediamine (OPD), m-phenylenediamine (MPD), p-phenylenediamine (PPD) and toluene-2,5-diamine (PTD). Additionally, 5-(4, 6-dichlorotriazinyl) aminofl...
Source: Journal of Food and Drug Analysis - March 21, 2019 Category: Food Science Source Type: research

Comparative quality of the forms of decoction pieces evaluated by multidimensional chemical analysis and chemometrics: Poria cocos, a pilot study
Publication date: Available online 21 March 2019Source: Journal of Food and Drug AnalysisAuthor(s): Li-Xia Zhu, Jun Xu, Yun Wu, Li-Fei Su, Kelly Yin Ching Lam, Elizabeth R. Qi, Xiao-Ping Dong, Hu-Biao Chen, Yu-De Liu, Zhong-Zhen ZhaoAbstractMany Chinese medicinal materials (CMMs) are parts of plants or fungi that have been processed into different physical forms, termed decoction pieces, that are typically boiled in water for consumption. One CMM may have several decoction pieces forms, e.g., slices, small cubes (dice), or grains. The specifications that have different morphological parameters (shape, size and thickness) f...
Source: Journal of Food and Drug Analysis - March 21, 2019 Category: Food Science Source Type: research

Proanthocyanidins from the stem bark of Rhus tripartita ameliorate methylgloxal-induced endothelial cell apoptosis
Publication date: Available online 17 March 2019Source: Journal of Food and Drug AnalysisAuthor(s): Ali S. Alqahtani, Wael M. Abdel-mageed, Abdelaaty A. Shahat, Mohammad K. Parvez, Mohammed S. Al-Dosari, Ajamaluddin Malik, Maged S. Abdel-Kader, Mansour S. AlsaidAbstractIn traditional Arabian medicine, the Rhus tripartita plant (family Anacardiaceae) has been used to treat inflammatory conditions. Although Rhus extracts have been reported for their cardioprotective effects, information regarding their active principle compounds remains insufficient. The present investigation was aimed at determining the antioxidant chemical...
Source: Journal of Food and Drug Analysis - March 18, 2019 Category: Food Science Source Type: research

Multi-residue analysis using liquid chromatography tandem mass spectrometry for detection of 20 coccidiostats in poultry, livestock, and aquatic tissues
In this study, we developed a novel analysis method based on liquid chromatography/tandem mass spectrometry (LC–MS/MS) to allow the simultaneous identification of 20 coccidiostats in eight matrix categories, including the muscles of chicken, swine, cow, and fish as well as chicken eggs, bovine milk, and porcine viscera. In the pretreatment procedure, acetonitrile/methanol (95:5, v/v) containing 1% formic acid, 5 g of sodium acetate, and 6.0 g of anhydrous magnesium sulfate was used for extraction, followed by a clean-up procedure using n-hexane saturated with ACN to facilitate the elimination of analytes from high lipi...
Source: Journal of Food and Drug Analysis - March 13, 2019 Category: Food Science Source Type: research

Potential prebiotics and their transmission mechanisms: Recent approaches
Publication date: Available online 4 March 2019Source: Journal of Food and Drug AnalysisAuthor(s): Ishu Khangwal, Pratyoosh ShuklaAbstractPrebiotics are non digestible carbohydrates which can be used as prime source of energy for gut microflora. These can be naturally occurring in fruit and vegetables or can be made synthetically by enzymatic digestions. New versatile sources of prebiotics had been found nowadays for economic commercialization. This review will decipher on highlighting the importance of prebiotics in immunomodulation and nutrient absorption abilities of gut, as it is important for anti-effective capacity o...
Source: Journal of Food and Drug Analysis - March 5, 2019 Category: Food Science Source Type: research

Determination of polycyclic aromatic hydrocarbons (PAHs) in cosmetic products by gas chromatography-tandem mass spectrometry
This study offers a sensitive and simple method to analyze 18 representative PAHs successfully and can be applied to cosmetic products and raw materials.Graphical abstract (Source: Journal of Food and Drug Analysis)
Source: Journal of Food and Drug Analysis - February 22, 2019 Category: Food Science Source Type: research

An ultra-rapid drug screening method for acetaminophen in blood serum based on probe electrospray ionization-tandem mass spectrometry
Publication date: Available online 22 February 2019Source: Journal of Food and Drug AnalysisAuthor(s): Kiyotaka Usui, Haruka Kobayashi, Yuji Fujita, Eito Kubota, Tomoki Hanazawa, Tomohiro Yoshizawa, Yoshito Kamijo, Masato FunayamaAbstractPoisoning incidents caused by drugs, accidental ingestion of poisons, attempted suicide, homicide, and exposure to toxic compounds occur frequently every year across the globe. This raises the need to rapidly identify toxic agents in poisoned patients in a clinical emergency setting. In addition, determining drug/poison concentration is undoubtedly necessary to arrive at a toxicological tr...
Source: Journal of Food and Drug Analysis - February 22, 2019 Category: Food Science Source Type: research

Psychobiotics in mental health, neurodegenerative and neurodevelopmental disorders
Publication date: Available online 10 February 2019Source: Journal of Food and Drug AnalysisAuthor(s): Li-Hao Cheng, Yen-Wenn Liu, Chien-Chen Wu, Sabrina Wang, Ying-Chieh TsaiAbstractPsychobiotics are a group of probiotics that affect the central nervous system (CNS) related functions and behaviors mediated by the gut-brain-axis (GBA) via immune, humoral, neural, and metabolic pathways to improve not only the gastrointestinal (GI) function but also the antidepressant and anxiolytic capacity. As a novel class of probiotics, the application of psychobiotics has led researchers to focus on a new area in neuroscience. In the p...
Source: Journal of Food and Drug Analysis - February 11, 2019 Category: Food Science Source Type: research

Revisit gut microbiota and its impact on human health and disease
Publication date: Available online 1 February 2019Source: Journal of Food and Drug AnalysisAuthor(s): Rui-xue Ding, Wei-Rui Goh, Ri-na Wu, Xi-qing Yue, Xue Luo, Thwe Khine Wei Wei, Jun-rui Wu, Yuan-Kun LeeAbstractTrillions of microbes have evolved with and continue to live on human beings. With the rapid advances in tools and technology in recent years, new knowledge and insight in cross-talk between the microbes and their hosts have gained. It is the aim of this work to critically review and summarize recent literature reports on the role of microbiota and mechanisms involved in the progress and development of major human...
Source: Journal of Food and Drug Analysis - February 2, 2019 Category: Food Science Source Type: research

Next generation probiotics in disease amelioration
Publication date: Available online 2 February 2019Source: Journal of Food and Drug AnalysisAuthor(s): Chih-Jung Chang, Tzu-Lung Lin, Yu-Ling Tsai, Tsung-Ru Wu, Wei-Fan Lai, Chia-Chen Lu, Hsin-Chih LaiAbstractStudies on the role of gut commensal bacteria in health development have rapidly attracted much more attention beyond the classical pathogens over the last decade. Many important reports have highlighted the changes in the gut microbiota (dysbiosis) are closely related to development of intra- and extra-intestinal, chronic inflammation related diseases such as colitis, obesity/metabolic syndromes, diabetes mellitus, li...
Source: Journal of Food and Drug Analysis - February 2, 2019 Category: Food Science Source Type: research

Current status of MALDI-TOF mass spectrometry in clinical microbiology
Publication date: Available online 31 January 2019Source: Journal of Food and Drug AnalysisAuthor(s): Tsung-Yun Hou, Chuan Chiang-Ni, Shih-Hua TengAbstractMass spectrometry (MS) is a type of analysis used to determine what molecules make up a sample, based on the mass spectrum that are created by the ions. Mass spectrometers are able to perform traditional target analyte identification and quantitation; however, they may also be used within a clinical setting for the rapid identification of bacteria. The causative agent in sepsis is changed over time, and clinical decisions affecting the management of infections are often ...
Source: Journal of Food and Drug Analysis - January 31, 2019 Category: Food Science Source Type: research

Direct injection high performance liquid chromatography coupled to data independent acquisition mass spectrometry for the screening of antibiotics in honey
Publication date: Available online 29 January 2019Source: Journal of Food and Drug AnalysisAuthor(s): Annie von Eyken, Daniel Furlong, Samareh Arooni, Fred Butterworth, Jean-François Roy, Jerry Zweigenbaum, Stéphane BayenAbstractThe targeted analysis of veterinary drug residues in honey traditionally involves a series of extraction and purification steps prior to quantification with high performance liquid chromatography coupled to high resolution or tandem mass spectrometry. These steps, designed to separate the target analytes from interferences, are generally time-consuming and costly. In addition, traditional cleanup...
Source: Journal of Food and Drug Analysis - January 30, 2019 Category: Food Science Source Type: research